Reference number
ISO 9504:1993
ISO 9504:1993
Metallurgical-grade fluorspar — Determination of antimony content — Solvent extraction atomic absorption spectrometric method
Edition 2
1993-04
Withdrawn
ISO 9504:1993
17233
Withdrawn (Edition 2, 1993)

Abstract

The principle of the method specified is to decompose a test portion by a mixture of nitric, hydrofluoric and perchloric acids, dissolving the salts in hydrochloric acid after evaporation to fumes of sulfuric acid, extracting the antimony from a dilute hydrochloric acid solution of the decomposed test portion into a solution of tri-n-octylphosphine oxide in 4-methyl-2-pentanone, aspirating the extract into the air/acetylene flame of an atomic absorption spectrometer, and measuring the absorbance at 217,6 nm. Applies to products having an antimony content equal to or greater than 0,001 % (m/m).

General information

  •  : Withdrawn
     : 1993-04
    : Withdrawal of International Standard [95.99]
  •  : 2
     : 7
  • ISO/TC 175
    73.080 
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